Abstract
Using an ion exchange membrane as a separator,the 2,2′-Dichlorohydrazobenzene is synthesized by the electrolytic reduction of o-chloronetrobenzene.The effects of electrode activation condition,current density,electrolyte temperature on electrolytic reduction are discussed.It was found that the optimum reaction temperature is 80 ℃.When the electrolyte concentration was 30% NaOH at the anode and 10% NaOH at the cathode,current density is 4.2A/dm2,the current efficiency reached 73% and yield is 83%.
Keywords
2, 2′-Dichlorohydrazobenzene, ion exchange membrane, electrolytic reduction, activation condition
Publication Date
2008-02-28
Online Available Date
2008-02-28
Revised Date
2008-02-28
Received Date
2008-02-28
Recommended Citation
Chao ZHANG, Pei-jin LI.
Synthesis of 2,2′-dichlorohydrazobenzene Using an Ion Exchange Membrane[J]. Journal of Electrochemistry,
2008
,
14(1): 61-65.
DOI: 10.61558/2993-074X.1864
Available at:
https://jelectrochem.xmu.edu.cn/journal/vol14/iss1/13
Included in
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