Synthesis of 2,2′-dichlorohydrazobenzene Using an Ion Exchange Membrane

Authors

Chao ZHANG, College of Materials Science and Engineering,Beijing University of Chemical Technology,Beijing 100029,China;
Pei-jin LI, College of Materials Science and Engineering,Beijing University of Chemical Technology,Beijing 100029,China;

Abstract

Using an ion exchange membrane as a separator,the 2,2′-Dichlorohydrazobenzene is synthesized by the electrolytic reduction of o-chloronetrobenzene.The effects of electrode activation condition,current density,electrolyte temperature on electrolytic reduction are discussed.It was found that the optimum reaction temperature is 80 ℃.When the electrolyte concentration was 30% NaOH at the anode and 10% NaOH at the cathode,current density is 4.2A/dm2,the current efficiency reached 73% and yield is 83%.

Keywords

2, 2′-Dichlorohydrazobenzene, ion exchange membrane, electrolytic reduction, activation condition

DOI Link

https://doi.org/10.61558/2993-074X.1864

Publication Date

2008-02-28

Online Available Date

2008-02-28

Revised Date

2008-02-28

Received Date

2008-02-28

Recommended Citation

Chao ZHANG, Pei-jin LI. Synthesis of 2,2′-dichlorohydrazobenzene Using an Ion Exchange Membrane[J]. Journal of Electrochemistry, 2008 , 14(1): 61-65.
DOI: 10.61558/2993-074X.1864
Available at: https://jelectrochem.xmu.edu.cn/journal/vol14/iss1/13

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