Abstract
In this work, the p-TSA doped and hierarchical dendritic nanostructured polyanilines (PANI) have been prepared by potentiostatic electropolymerization without using any templates at room temperature. The mechanism of the polymerization has been discussed according to the electrodeposition curves. Scanning electron microscopy (SEM) and transmission electron microscopy (TEM) were employed to confirm the formation of uniform hierarchical dendritic structure on PANI. UV-Vis spectroscopy (UV-Vis) and infrared spectroscopy (FTIR) proved that the prepared PANI is in the form of emeraldine salt. The templateless electrodeposition method is simple, easy to operate, can be applied to fabricate other nanostructures of conducting polymers.
Graphical Abstract
Publication Date
2013-04-28
Online Available Date
2012-01-15
Revised Date
2012-01-05
Received Date
2011-11-17
Recommended Citation
Shao-Huang WENG, Jian-Zhang ZHOU, Zhong-Hua LIN, Xin-Hua LIN.
Electrochemical synthesis of hierarchical dendritic polyaniline nanostructures[J]. Journal of Electrochemistry,
2013
,
19(2): Article 16.
DOI: 10.61558/2993-074X.2945
Available at:
https://jelectrochem.xmu.edu.cn/journal/vol19/iss2/16
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